Acid-catalysed cleavage of a 1,3-photoadduct of benzene and cis-3,4-dichlorocyclobutene: X-ray structure of 3,4-dichlorotricyclo[4,3,1, 02,5]dec-8-en-10-yl p-nitrobenzoate

Gollapudy Subrahmanyam; Rangaswamy Srinivasan; Sam J. La Placa; James E. Weidenborner

doi:10.1039/C3975000231a

Journal of the Chemical Society, Chemical Communications

Paper

01 Jan 1975

Acid-catalysed cleavage of a 1,3-photoadduct of benzene and cis-3,4-dichlorocyclobutene: X-ray structure of 3,4-dichlorotricyclo[4,3,1, 0^2,5]dec-8-en-10-yl p-nitrobenzoate

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Abstract

The structure of the alcohol, obtained from acid treatment of the photoadduct (1) of benzene and cis-3,4-dichlorobutene, was established as (2) by a single crystal X-ray structure analysis of its p-nitrobenzoate racemate (3).

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